PENETRATION GRADE BITUMEN 

The distillation process starts in the refinery where the crude oil is heated and delivered to an atmospheric distillation column (ADC) where the lighter fractions are vaporized and drawn off, leaving a residue of heavy oils and bitumen.

 

The crude oil is pumped into the ADC at temperatures between 300-350 °C (575-660°F) at the bottom of the tower.  At these temperatures, the crude oil is already a mixture of liquid and vapor.  The vapors rise up the ADC through holes in trays which are constructed throughout the distillation column.  The temperature decreases with the height of the ADC, allowing the vapors to condense according to different boiling ranges.

 

In this way the lighter, lower boiling fractions rise to the top, while heavier fractions are taken out from trays as side streams part way up. The heaviest fraction, the so-called long residue, leaves from the bottom.  The top fraction is LPG (liquefied petroleum gas) followed by naphtha, paraffin, gas-oil, and heavy distillates.

 

The long residue is then further distilled under vacuum in the vacuum distillation column (VDC).  In the VDC, the long residue is separated into heavy gas-oil, heavy distillates, and a soft residue.  This residue is termed short residue and can be used as bitumen feedstock.  The penetration of the short residue is variable and depends on the nature of the crude oil and the vacuum distillation conditions.  The penetration typically runs from 10 to 500.  Different penetration (pen) levels can be obtained by blending different short residues in the right proportion or by direct distilling.  Bitumen products produced this way are referred to as straight-run bitumen.

 

 

CUTBACK BITUMEN

 

Cutback bitumen has been blended with a volatile oil so that when the volatiles have evaporated with time the bitumen will eventually revert to its original viscosity.

 

Time being the critical factor, it may take many months or even years before the cutback mixture regains the viscosity of the original bitumen.

 

The solvents used for dilution are distillates of varying volatiles. After bitumen cutback has been applied, the diluents evaporate and leave the residual bitumen in contact with the aggregate.  In this process the diluents do not play any part in the function of the binder.  However, the type and amount of diluents used decide the rate of solvent evaporation and the curing rate of bitumen cutback.

 

The tables below show the specifications of the specific grades of bitumen that we provide.

 

PENETRATION BITUMEN    60/70

SPECIFICATIONS

TEST RESULT

TEST METHOD

Specific Gravity at 25/25 (°C)

1.01/1.06

D - 70

Penetration at 25 (°C)

60/70

D - 5

Softening Point (°C)

46/56

D - 36

Ductility at 25 (°C) 

100 min.

D -113

Loss on Heating PCT (WT) %

0.2 max.

D - 6

Drop in Penetration after Heating PCT. (WT) %

20 max.

D - 6/D - 5

Flash Point (°C). 

250 min.

D - 92

Solubility in CS2 (WT ) % 

99.5 min.

D - 4

Spot Test

Negative

* A.A.S.H.O. T102

(°C) = Degrees Celsius   *AMERICAN ASSOCIATION OF STATE HIGHWAY OFFICIALS
PENETRATION BITUMEN     85/100

SPECIFICATIONS

TEST RESULT

TEST METHOD

Specific Gravity at 25/25 (°C)

1.00/1.05

D - 70

Penetration at 25 (°C)

85/100

D - 5

Softening Point (°C) 

45/ 52

D - 36

Ductility at 25 (°C) CMS.

100 min.

D - 113

Loss on Heating PCT (WT) %

0.5 max.

D - 6

Drop in Penetration after Heating PCT. (WT) %

20 max.

D - 6/D - 5

Flash Point (°C)

225 min.

  D - 92

Solubility in CS2 (WT) %.

99.5 max.

D - 4

O.M. Insoluble in CS2 (WT) %

0.2 max.

D - 4

Spot Test 

Negative

*A.A.S.H.O.T102

(°C) = Degrees Celsius   *AMERICAN ASSOCIATION OF STATE HIGHWAY OFFICIALS
CUTBACK BITUMEN  MC-70

SPECIFICATIONS

TEST RESULT

TEST METHOD

Sample Amount From 0.6 litre per m2 to 1.2 litre/m2
Spraying/Sample Temp. 60 - 80 (°C)

Kinematic Viscosity at 60 (°C)

Cst 70-140

D - 2170

Flash point (Tag open - Cup ) (°C) 

66 min.

D - 3143

Distillation % by Vol. of Total Distillate to 360  (°C) Method: D - 402

190 (°C)

-

 

225 (°C)

(vol) % 10 -50

 

260 (°C) (vol) % 40 -80  

316 (°C)

(vol) % 80 -95

 

Residue from Distillation 

Ductility at 25 (°C) Cms. 55 min D-113
Penetration at 25 (°C) 90-180 D-5
(°C) = Degrees Celsius  
CUTBACK BITUMEN  MC-30

SPECIFICATIONS

TEST RESULT

TEST METHOD

Sample Amount From 0.6 litre per m2 to 1.2 litre/m2
Spraying/Sample Temp. 45 - 65 (°C)

Kinematic Viscosity at 60 (°C)

Cst 30-60

D - 2170

Flash point (Tag open - Cup ) (°C) 

66 min.

D - 3143

Distillation % by Vol. of Total Distillate to 360  (°C) Method: D - 402

190 (°C)

(vol)% 0-15

 

225 (°C)

(vol) % 15 -60

 

260 (°C) (vol) % 50 -85  

316 (°C)

(vol) % 80 -100

 

Residue from Distillation 

Ductility at 25 (°C) Cms. 50 min D-113
Penetration at 25 (°C) 90-180 D-5
(°C) = Degrees Celsius  
CUTBACK BITUMEN  MC-250

SPECIFICATIONS

TEST RESULT

TEST METHOD

Kinematic Viscosity at 60 (°C)

Cst 250-500

D - 2170

Flash point (Tag open - Cup ) (°C) 

66 min.

D - 3143

Distillation

test

D - 402

225 (°C)

(vol)% 10 max.

 

260 (°C)

(vol) % 15 -55

 

326 (°C)

(vol) % 60 - 87

 

Residue from Distillation 

Ductility at 25 (°C) Cms. 100 min D-113
Penetration at 25 (°C) 120-250 D-5
Solubility in trichloroethylen (wt)% 99.0 min. D-2042
Water Content (vol)% 0.2 max. D-95

360 (°C)

(vol) % 67 min.

 

(°C) = Degrees Celsius  
BLOWN (Oxidized) BITUMEN     R 90/15

SPECIFICATIONS

TEST RESULT

TEST METHOD

Specific Gravity at 25/25 (°C)

1.05 approx.

D - 70

Penetration at 25 (°C) 

10/20

D - 5

Softening Point (°C) 

85/95

D - 36

Ductility at 25 (°C) 

1.5 min.

D - 113

Loss on Heating (WT) % 

0.2 max.

D - 6

Flash Point (°C)

225 max.

D - 92

Solubility in CS2 (WT) %

99 min.

D - 4

(°C) = Degrees Celsius  
BLOWN (Oxidized) BITUMEN     R 85/25

SPECIFICATIONS

TEST RESULT

TEST METHOD

Specific Gravity at 25/5 (°C) 

1.05 approx.

D - 70

Penetration at 25 (°C) 

20/30

D - 5

Softening Point (°C) 

80/90

D - 36

Ductility at 25 (°C) 

3 min.

D - 113

Loss on Heating (WT) % 

0.2 max.

D - 6

Flash Point (°C)

225 max.

D - 92

Solubility in CS2 (WT) %

99 min.

D - 4

(°C) = Degrees Celsius  
PENETRATION BITUMEN     180/200

SPECIFICATIONS

TEST RESULT

TEST METHOD

Penetration at 25 (°C)

180/200

D - 5

Softening Point (°C) 

35/ 45

D - 36

Ductility at 25 (°C) CMS.

50 min.

D - 113

Loss on Heating PCT (WT) %

1.0 max.

D - 6

Drop in Penetration after Heating PCT. (WT) %

35

D - 5

Flash Point (°C)

200 min.

  D - 92

Solubility in CS2 (WT) %.

99 min.

D - 4

(°C) = Degrees Celsius   *AMERICAN ASSOCIATION OF STATE HIGHWAY OFFICIALS
PENETRATION BITUMEN     100/120

SPECIFICATIONS

TEST RESULT

TEST METHOD

Specific Gravity at 25/25 (°C)

1.01/1.04

D - 70

Penetration at 25 (°C)

100/120

D - 5

Softening Point (°C) 

42/ 49

D - 36

Ductility at 25 (°C) CMS.

100 min.

D - 113

Loss on Heating PCT (WT) %

0.2 max.

D - 6

Drop in Penetration after Heating PCT. (WT) %

20 max.

D - 5

Flash Point (°C)

250

  D - 92

Solubility in CS2 (WT) %.

99.5 max.

D - 4

O.M. Insoluble in CS2 (WT) %

0.2 max.

D - 4

(°C) = Degrees Celsius   *AMERICAN ASSOCIATION OF STATE HIGHWAY OFFICIALS
PENETRATION BITUMEN     80/100

SPECIFICATIONS

TEST RESULT

TEST METHOD

Specific Gravity at 25/25 (°C)

1.00/1.05

D - 70

Penetration at 25 (°C)

80/100

D - 5

Softening Point (°C) 

45/ 52

D - 36

Ductility at 25 (°C) CMS.

100 min.

D - 113

Loss on Heating PCT (WT) %

0.5 max.

D - 6

Drop in Penetration after Heating PCT. (WT) %

20 max.

D - 5

Flash Point (°C)

225 min.

  D - 92

Solubility in CS2 (WT) %.

99.5 max.

D - 4

O.M. Insoluble in CS2 (WT) %

0.2 max.

D - 4

(°C) = Degrees Celsius   *AMERICAN ASSOCIATION OF STATE HIGHWAY OFFICIALS
PENETRATION BITUMEN    6/12

SPECIFICATIONS

TEST RESULT

TEST METHOD

Penetration at 25 (°C)

6/12

D - 5

Softening Point (°C)

60/90

D - 36

Ductility at 25 (°C) CMS

-

D - 113

Loss on Heating PCT (WT) %

0.1 max.

D - 6

Drop in Penetration after Heating PCT. (WT) %

-

D - 5

Flash Point (°C)

290 min.

D - 92

Solubility in CS2 (WT) %

99 min.

D - 2042

(°C) = Degrees Celsius  
PENETRATION BITUMEN    10/20

SPECIFICATIONS

TEST RESULT

TEST METHOD

Penetration at 25 (°C)

10/20

D - 5

Softening Point (°C)

65/75

D - 36

Ductility at 25 (°C) CMS

5

D - 113

Loss on Heating PCT (WT) %

0.5 max.

D - 6

Drop in Penetration after Heating PCT. (WT) %

25

D - 5

Flash Point (°C)

250 min.

D - 92

Solubility in CS2 (WT) %

99 min.

D - 2042

(°C) = Degrees Celsius  
PENETRATION BITUMEN    20/30

SPECIFICATIONS

TEST RESULT

TEST METHOD

Penetration at 25 (°C)

20/30

D - 5

Softening Point (°C)

58/68

D - 36

Ductility at 25 (°C) CMS

25

D - 113

Loss on Heating PCT (WT) %

0.5 max.

D - 6

Drop in Penetration after Heating PCT. (WT) %

25

D - 5

Flash Point (°C)

250 min.

D - 92

Solubility in CS2 (WT) %

99 min.

D - 2042

(°C) = Degrees Celsius  
PENETRATION BITUMEN    30/40

SPECIFICATIONS

TEST RESULT

TEST METHOD

Specific Gravity at 25/25 (°C)

1.01/1.06

D - 70

Penetration at 25 (°C)

30/40

D - 5

Softening Point (°C)

55/63

D - 36

Ductility at 25 (°C) CMS

100 min.

D - 113

Loss on Heating PCT (WT) %

0.2 max.

D - 6

Drop in Penetration after Heating PCT. (WT) %

20 max.

D - 5

Flash Point (°C)

250 min.

D - 92

Solubility in CS2 (WT) %

99.5 max.

D - 4

Spot Test

Negative

* A.A.S.H.O. T102

(°C) = Degrees Celsius   *AMERICAN ASSOCIATION OF STATE HIGHWAY OFFICIALS
PENETRATION BITUMEN    40/50

SPECIFICATIONS

TEST RESULT

TEST METHOD

Specific Gravity at 25/25 (°C)

1.01/1.06

D - 70

Penetration at 25 (°C)

40.50

D - 5

Softening Point (°C)

52/60

D - 36

Ductility at 25 (°C) CMS

100 min.

D - 113

Loss on Heating PCT (WT) %

0.2 max.

D - 6

Drop in Penetration after Heating PCT. (WT) %

20 max.

D - 6 / D - 5

Flash Point (°C)

250 min.

D - 92

Solubility in CS2 (WT) %

99.5 min.

D - 4

Spot test

Negative

*A.A.S.H.O.T102

(°C) = Degrees Celsius   *AMERICAN ASSOCIATION OF STATE HIGHWAY OFFICIALS